刘永利,赵振霞,苏建,王敏,冯丽.三七粉质量评价研究[J].中国药事,2017,(4):407-411 |
三七粉质量评价研究 |
Quality Evaluation of Panax Notoginseng Powder |
投稿时间:2016-10-20 |
DOI:10.16153/j.1002-7777.2017.04.010 |
中文关键词: 三七 三七粉 法定标准检验 质量评价 探索性研究 三七茎叶 |
英文关键词: Panax notoginseng Panax notoginseng powder legal standard test quality evaluation exploratory study leaves of Panax notoginseng |
基金项目:十二五国家科技重大专项“中药质量安全检测和风险控制技术平台”课题(编号2014ZX09304307-002) |
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中文摘要: |
目的:对市场上三七粉质量进行评价与分析,为药品监督管理提供技术依据。方法:用现行标准检验样品;采用薄层色谱法、超高效液相色谱法、电感耦合等离子体质谱法等分析手段,从有效成分定性定量、原料来源及重金属检测等方面开展探索性研究,分析三七粉内在质量。结果:现行标准检验合格率为100%,探索性研究可发现三七茎叶原料。结论:三七粉整体质量状况较好,个别批次样品存在非法掺加三七茎叶现象。 |
英文摘要: |
Objective: To evaluate and analyze the quality of Panax notoginseng powder at market and provide technical references for drug administration. Methods: Samples were tested with current standard and analyzed by the following methods, such as TLC, UPLC and ICP-MS. Exploratory studies were developed for qualitative and quantitative determination of active ingredients, source of raw materials and heavy metal testing and so on to analyze the intrinsic quality of Panax notoginseng powder. Results: Qualified sample rate was 100% according to the current standard, the exploratory studies could identify raw materials of leaves of Panax notoginseng.Conclusion: The overall quality of domestic Panax notoginseng powder is satisfying except for few batches of samples containing illegally added leaves of Panax notoginseng. |
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