| 马敏,马鑫,周瑞雪.少腹逐瘀丸多种挥发性成分同时检测的方法研究[J].中国药事,2018,32(7):919-926 |
| 少腹逐瘀丸多种挥发性成分同时检测的方法研究 |
| On the Method for Simultaneous Determination of Multiple Volatile Components in Shaofu Zhuyu Pill |
| 投稿时间：2018-01-22 |
| DOI：10.16153/j.1002-7777.2018.07.013 |
| 中文关键词: 中成药 桂皮醛 反式茴香脑 蒿本内酯 气相色谱法 少腹逐瘀丸 |
| 英文关键词: Chinese patent medicine cinnamaldehyde cis-anethol ligustilide gas chromatography Shaofu Zhuyu Pill |
| 基金项目:2014年国家食品药品监督管理总局国家评价性抽验项目-少腹逐瘀丸（编号食药监办药化监［2014］61号） |
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| 中文摘要: |
| 目的：建立同时测定少腹逐瘀丸中桂皮醛、反式茴香脑、蒿本内酯含量的方法。方法：采用气相色谱法、DM-5毛细柱、程序升温、FID检测器进行检测。结果：肉桂中桂皮醛、小茴香中反式茴香脑、当归与川芎中蒿本内酯在各自的线性范围内与其峰面积呈良好的线性关系；平均加样回收率在98.29%~99.02%，RSD均符合规定。结论：该方法准确、简便、快速，可用于少腹逐瘀丸中多味药材的多种挥发性成分的检测。 |
| 英文摘要: |
| Objective:To establish a method for simultaneous determination of cinnamaldehyde, cis-anethol, ligustilide in Shaofu Zhuyu Pill. Methods:Gas chromatography (GC) was conducted on a DM-5 capillary column with FID detector under programmed temperature. Results:Cinnamaldehyde in cinnamon, cis-anethol in fennel, ligustilide in angelica and ligusticum wallichii all had a good linear relationship with their peak area. The average recovery rate was between 98.29% and 99.02%. RSD was in accordance with the regulations. Conclusion:The method is accurate, simple, rapid and can be used for the determination of multiple volatile components in Shaofu Zhuyu Pills. |
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